Iluphu yesampula ye-SS ibheka enye i-Agilent autosampler injector yamanuwali

Ama-loop amasampula ahlanganisa ishubhu nokufakwa. Yonke iluphu yesampula ifakwe izinto ezi-2, ezilungisa ishubhu ezindaweni ezimbili ukuze kuxhunywe okuthembeke kakhudlwana. Kukhona ukufakwa kwensimbi okubili kuzo zombili iziphetho zamasampula ensimbi engagqwali, futhi ukufakwa kwe-PEEK kuyiziphetho zombili zesampuli yeluphu ye-PEEK. I-Chromasir ikhiqiza uhla lwamasampuli oluluphu lwekhwalithi ephezulu. Zenziwe ngensimbi engagqwali engu-316L noma ukulunguza, ezifanele ama-Agilent autosamplers noma ama-injection manual. Amandla e-loop eyisampula ayahluka ukusuka ku-5µL ukuya ku-100µL. Izihibe zesampula zensimbi engagqwali zihlanzwe nge-ultrasonically. Amashubhu amasampula ensimbi engagqwali amaluphu awanayo i-burr futhi asikwe ngokuqondile ukuze kuqinisekiswe ukuthi i-solvent igeleza kahle kuvalvu. Amaluphu esampula e-PEEK angaba enye yesampula yamaluphu ensimbi engagqwali. Isampula ye-PEEK loop yokusika ihlanzekile futhi iqondile isiza ukuxhumeka kwevolumu efile ephansi. Futhi ayizincibilikisi eziningi zezinto eziphilayo futhi amelana nezincibilikisi zebhayoloji. Amasampula amaluphu ethu angaqinisekisa ukuxhumana okulula nokuthembekile ohlelweni lwe-HPLC.